4746-97-8
- Product Name：1,4-Cyclohexanedione Monoethylene Acetal
- Molecular Formula：C8H12O3
- Purity：99%
- Molecular Weight：156.181
Product Details
pd_meltingpoint:70-73 °C(lit.)
Appearance:off-white crystalline
Purity:99%
Manufacturer supply good quality 1,4-Cyclohexanedione Monoethylene Acetal 4746-97-8 with stock
- Molecular Formula:C8H12O3
- Molecular Weight:156.181
- Appearance/Colour:off-white crystalline
- Vapor Pressure:0.00776mmHg at 25°C
- Melting Point:70-73 °C(lit.)
- Refractive Index:1.489
- Boiling Point:268.3 °C at 760 mmHg
- Flash Point:106.7 °C
- PSA：35.53000
- Density:1.16 g/cm3
- LogP:0.87260
1,4-Dioxaspiro[4.5]decan-8-one(Cas 4746-97-8) Usage
|
Purification Methods |
Recrystallise it from pet ether. It sublimes slowly on attempted distillation. Also purify it by dissolving it in Et2O and adding pet ether (b 60-80o) until turbid and cooling. [Gardner et al. J Am Chem Soc 22 1206 1957, Britten & Lockwood J Chem Soc Perkin Trans 1 1824 1974.] [Beilstein 19/4 V 93.] |
InChI:InChI=1/C8H12O3/c9-7-1-3-8(4-2-7)10-5-6-11-8/h1-6H2
4746-97-8 Relevant articles
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Paragraph 0150; 0259-0260; 0262-0263, (2020/08/30)
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Paragraph 0016-0021; 0023; 0024; 0026; 0027, (2019/04/04)
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4746-97-8 Process route
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67-51-6
3,5-dimethyl-1H-pyrazole
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4-hydroxycyclohexane mono-ketal
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4-hydroxycyclohexane mono-ketal
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4746-97-8
cyclohexanedione monoethylene ketal
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637-88-7
1,4-Cyclohexanedione
| Conditions | Yield |
|---|---|
|
In
dichloromethane; ethyl acetate;
|
91% |
-
![1,4,9,12-Tetraoxa-dispiro[4.2.4.2]tetradecane](/upload/2026/5/5f3d9966-a581-460e-a96e-eebe91f90ae1.png)
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183-97-1
1,4,9,12-Tetraoxa-dispiro[4.2.4.2]tetradecane
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-
4746-97-8
cyclohexanedione monoethylene ketal
-
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637-88-7
1,4-Cyclohexanedione
| Conditions | Yield |
|---|---|
|
With
formaldehyd; silica gel; iron(III) chloride;
at 20 ℃;
for 0.416667h;
|
22 % Chromat. 58% |
4746-97-8 Upstream products
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14160-65-7
ethyl 8-oxo-1,4-dioxaspiro[4.5]decane-7-carboxylate
4746-97-8 Downstream products
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125541-17-5
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155778-83-9
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94112-58-0
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