4101-68-2
- Product Name：1,10-Dibromodecane
- Molecular Formula：C10H20Br2
- Purity：99%
- Molecular Weight：300.077
Product Details
pd_meltingpoint:25-27 °C(lit.)
Appearance:beige to brown crystalline low melting mass
Purity:99%
Cost-effective and customizable 1,10-Dibromodecane 4101-68-2 for sale
- Molecular Formula:C10H20Br2
- Molecular Weight:300.077
- Appearance/Colour:beige to brown crystalline low melting mass
- Vapor Pressure:0.00233mmHg at 25°C
- Melting Point:25-27 °C(lit.)
- Refractive Index:n20/D 1.4912(lit.)
- Boiling Point:297.9 °C at 760 mmHg
- Flash Point:153.4 °C
- PSA：0.00000
- Density:1.364 g/cm3
- LogP:4.89700
1,10-Dibromodecane(Cas 4101-68-2) Usage
InChI:InChI=1/C10H20Br2/c11-9-7-5-3-1-2-4-6-8-10-12/h1-10H2
4101-68-2 Relevant articles
-
Taylor
, p. 2068 (1958)
-
Asymmetric synthesis and biological evaluation of natural or bioinspired cytotoxic C 2-symmetrical lipids with two terminal chiral alkynylcarbinol pharmacophores
Listunov, Dymytrii,Fabing, Isabelle,Saffon-Merceron, Nathalie,Gaspard, Hafida,Volovenko, Yulian,Maraval, Valérie,Chauvin, Remi,Génisson, Yves
, p. 5386 - 5394 (2015)
Bidirectional syntheses of C2-symmetrica...
Acid monolayer functionalized iron oxide nanoparticles as catalysts for carbohydrate hydrolysis
Ikenberry, Myles,Pena, Leidy,Wei, Daming,Wang, Hongwang,Bossmann, Stefan H.,Wilke, Trenton,Wang, Donghai,Komreddy, Venugopal R.,Rillema, D. Paul,Hohn, Keith L.
, p. 836 - 843 (2014)
Superparamagnetic iron oxide nanoparticl...
Self-aggregation of synthesized novel bolaforms and their mixtures with sodium dodecyl sulfate (SDS) and cetyltrimethylammonium bromide (CTAB) in aqueous medium
Maiti, Kajari,Mitra, Debolina,Mitra, Rajendra N.,Panda, Amiya K.,Das, Prasanta K.,Rakshit, Animesh K.,Moulik, Satya P.
, p. 7499 - 7508 (2010)
Bolaforms B1, B2, and B3 of the formulas...
PROCESS FOR THE PREPARATION OF ORGANIC BROMIDES
-
Paragraph 00169; 00172, (2017/07/28)
The present invention provides a process...
Silver-Catalyzed Decarboxylative Bromination of Aliphatic Carboxylic Acids
Tan, Xinqiang,Song, Tao,Wang, Zhentao,Chen, He,Cui, Lei,Li, Chaozhong
supporting information, p. 1634 - 1637 (2017/04/11)
The silver-catalyzed Hunsdiecker bromina...
Catalytic Access to Alkyl Bromides, Chlorides and Iodides via Visible Light-Promoted Decarboxylative Halogenation
Candish, Lisa,Standley, Eric A.,Gómez-Suárez, Adrián,Mukherjee, Satobhisha,Glorius, Frank
supporting information, p. 9971 - 9974 (2016/07/19)
Herein is reported the catalytic, visibl...
Process intensification-assisted conversion of α,ω-alkanediols to dibromides
Mekala, Shekar,Hahn, Roger C.
supporting information, p. 630 - 632 (2015/03/03)
The increasingly widespread applications...
4101-68-2 Process route
-
-
112-47-0
1,10-Decanediol
-
-
4101-68-2
1,10-dibromodecane
| Conditions | Yield |
|---|---|
|
With
hydrogen bromide;
In
octane; water;
at 145 ℃;
for 7h;
Dean-Stark;
|
91% |
|
With
hydrogen bromide;
In
water;
at 100 ℃;
for 48h;
|
86% |
|
With
hydrogen bromide;
In
water;
at 100 ℃;
for 48h;
|
80% |
|
With
sulfuric acid; hydrogen bromide;
|
|
|
With
sulfuric acid; sodium bromide;
|
|
|
With
hydrogen bromide;
at 60 ℃;
|
|
|
With
hydrogen bromide;
at 100 ℃;
|
|
|
With
hydrogen bromide;
|
|
|
With
hydrogen bromide;
at 95 ℃;
anschliessendes Erhitzen im HBr-Strom auf 135grad;
|
|
|
Multi-step reaction with 2 steps
1: tetrahydrofuran / 0.25 h / Ambient temperature
2: LiBr / tetrahydrofuran; hexamethylphosphoric acid triamide / 4 h / Heating
With
lithium bromide;
In
tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide;
|
-
-
2834-05-1
11-bromoundecanoic acid
-
-
4101-68-2
1,10-dibromodecane
| Conditions | Yield |
|---|---|
|
With
bromine; dibromoisocyanuric acid;
In
dichloromethane;
at 20 ℃;
for 4h;
UV-irradiation;
|
85% |
|
With
silver triflate-bis(1,10-phenanthroline) complex; dibromoisocyanuric acid;
In
1,2-dichloro-ethane;
at 40 ℃;
for 120h;
Inert atmosphere;
Schlenk technique;
|
56% |
|
With
[4,4′-bis(1,1-dimethylethyl)-2,2′-bipyridine-N1,N1′]bis{3,5-difluoro-2-[5-(trifluoromethyl)-2-pyridinyl-κN]phenyl-κC}iridium(III) hexafluorophosphate; caesium carbonate; Diethyl 2-bromomalonate;
In
chlorobenzene;
at 20 ℃;
for 4h;
Inert atmosphere;
Irradiation;
|
50% |
|
11-bromoundecanoic acid;
With
mercury(II) oxide;
In
tetrachloromethane;
at 114.84 ℃;
for 0.5h;
Darkness;
With
bromine;
In
tetrachloromethane;
|
4101-68-2 Upstream products
-
112-47-0
1,10-Decanediol
-
4224-70-8
6-bromohexanoic acid
-
818-88-2
sebacic acid mono methyl ester
-
111-24-0
1,5-dibromo-pentane
4101-68-2 Downstream products
-
6266-40-6
decamethylene bis(pyridinium bromide)
-
6275-34-9
4,4'-dimethyl-1,1'-decanediyl-bis-pyridinium; dibromide
-
1465-74-3
1,10-bis(isoquinolinium)decane dibromide
-
6275-38-3
3,3'-dimethyl-2,2'-decanediyl-bis-isoquinolinium; dibromide
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-
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